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Intercomparison exercises: A requirement for accurate and precise analytical data
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نویسنده
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siddique n. ,waheed s.
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منبع
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journal of the chemical society of pakistan - 2011 - دوره : 33 - شماره : 6 - صفحه:839 -845
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چکیده
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External evaluation of laboratory results and procedures can be carried out by participation in intercomparison exercises. the results of the international atomic energy agency - marine environmental laboratory (iaea-mel),monaco intercomparsion exercise iaea-158,marine sediment are presented and discussed in this paper. using four different irradiation protocols instrumental neutron activation analysis (inaa) was used to quantify al,as,br,ce,co,cr,cs,eu,fe,hf,k,la,lu,mn,na,nd,rb,sb,sc,se,sm,ta,tb,th,v,yb and zn in this reference material (rm). iaea-405 (estuarine sediment) and iaea-sl1 (lake sediment) were used as compatible matrix rms for quality assurance (qa) purposes. the z-scores showed our results to be in very good agreement with the iaea certified values. furthermore the iaea placed our laboratory in group 1 for having = 90% of the data with acceptable z-scores.
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آدرس
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chemistry division,directorate of science,pakistan institute of nuclear science and technology (pinstech) p.o nilore, Pakistan, chemistry division,directorate of science,pakistan institute of nuclear science and technology (pinstech) p.o nilore, Pakistan
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Authors
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