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Synthesis,crystal structure and fungicidal activity of 3-(((4-Cyclopropyl-5-Methyl- 4H-1,2,4-Triazol-3-yl)Thio)Methyl)Benzonitrile H2O (1:1) solvent
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نویسنده
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jin j.-z. ,sun n.-b.
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منبع
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journal of the chemical society of pakistan - 2013 - دوره : 35 - شماره : 3 - صفحه:955 -959
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چکیده
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The title compound (c14h14n4s· h2o) were synthesized and recrystallized from ethanol. the compound was characterized by 1h nmr,elemental analyses and x-ray diffraction. the compound crystallized in the monoclinic space group p2(1)/c with a = 11.289(2),b = 15.675(3),c = 8.4835(17) å,α = 90,β = 104.65(3),γ =90°,v = 1452.4(5) å3,z = 4 and r = 0.0333 for 2545 observed reflections with i > 2σ(i). x-ray analysis reveals that not only intermolecular o-h···n interactions. the biological activities results showed that the title compound exhibited significant fungicidal activity towards six test fungi.
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کلیدواژه
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4-triazole; Antifungal activity; Cyclopropane; Synthesis
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آدرس
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college of biology and environmental engineering,zhejiang shuren university,hangzhou 310015, China, college of biology and environmental engineering,zhejiang shuren university,hangzhou 310015, China
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Authors
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