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Determination of cyclopiazonic acid in Chinese yellow wine by high-performance liquid chromatography–triple quadrupole mass spectrometry
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نویسنده
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peng q. ,xing w. ,xu q. ,chen j. ,yu h. ,chen f. ,li b. ,xu x. ,wang z. ,tian r. ,sun j. ,zou h.j. ,mo y. ,xie g.
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منبع
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journal of the chemical society of pakistan - 2017 - دوره : 39 - شماره : 3 - صفحه:484 -487
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چکیده
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Summary: we developed a detection method of cyclopiazonic acid (cpa),a mycotoxin in chinese yellow rice wine,based on high-performance liquid chromatography and triple quadrupole mass spectrometry. under optimized conditions,the limit of detection was 50 µg/l. cpa recovery rates in cpa-spiked chinese yellow rice wine were 80.1% and 85.1% at 25 µg/l and 1,050 µg/l cpa,respectively (r > 0.9994). the relative standard deviation was 6.21–9.17%. our developed method represents a rapid and accurate detection tool of cpa meeting minimum residue measurement requirements in chinese yellow rice wine. the method will be widely available as a reference and be employed for chinese official regulatory control purposes.
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کلیدواژه
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Cyclopiazonic acid; HPLC/QQQ MS; Rice Wine
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آدرس
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school of life sciences,shaoxing university,shaoxing, China, school of life sciences,shaoxing university,shaoxing, China, school of life sciences,shaoxing university,shaoxing, China, school of life sciences,shaoxing university,shaoxing, China, school of life sciences,shaoxing university,shaoxing, China, shaoxing testing institute of quality technical supervision,shaoxing, China, shaoxing testing institute of quality technical supervision,shaoxing, China, school of life sciences,shaoxing university,shaoxing, China, school of life sciences,shaoxing university,shaoxing, China, school of life sciences,shaoxing university,shaoxing, China, school of life sciences,shaoxing university,shaoxing, China, national engineering research center for chinese rice wine,china shaoxing rice wine group co.,ltd,shaoxing, China, school of life sciences,shaoxing university,shaoxing, China, national engineering research center for chinese rice wine,china shaoxing rice wine group co.,ltd,shaoxing, China
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Authors
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