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preparation and characterization of nano-zno catalyst and its application insynthesis of2-amino-3-phenylsulfonyl-4-aryl-4h-benzo[h]chromen derivatives
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نویسنده
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jodaian vida ,sadeghi bahareh
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منبع
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journal of applied chemical research - 2022 - دوره : 16 - شماره : 2 - صفحه:19 -30
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چکیده
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An efficient and environmentally adapted synthesis of 2-amino-3-phenylsulfonyl-4-aryl-4h-benzo[h]chromenderivatives by condensation of a wide range of aryl aldehydes, α-naphthol and (phenylsulfonyl)acetonitrile using a catalytic amount of nano-znounder solvent-free condition is explained. this catalyst was characterized by scanning electron microscopy (sem), fourier transform infrared spectroscopy (ft-ir),x-ray diffraction spectroscopy (edx)and thermogravimetric analysis (tg).as aresult, 2-amino-3-phenylsulfonyl-4-aryl-4h-benzo[h]chromens were produced under facile conditions in high yield (89-96%) and high rate (8-15 min) using nano-zno as a recyclable catalyst.
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کلیدواژه
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nano-zno ,nanocatalyst ,(phenylsulfonyl)acetonitrile ,solid acid ,α-naphthol،
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آدرس
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islamic azad university, islamshahrbranch, department of chemistry, iran, islamic azad university, central tehran branch, 2department of chemistry, iran
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پست الکترونیکی
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bsadeghi_4696@yahoo.com
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Authors
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