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Application of 2-methylpyridinum p-toluenesulfonate ([2- MPy][p-TSA]) as an efficient catalyst for the one-pot synthesis of hexahydroquinoline-3-carboxamides
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نویسنده
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asadi matin ,mokhtary masoud
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منبع
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journal of applied chemical research - 2018 - دوره : 12 - شماره : 4 - صفحه:78 -86
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چکیده
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2-methylpyridinum p-toluenesulfonate ([2-mpy][p-tsa]) as a novel room temperature ionic liquid was synthesized and evaluated as a recoverable catalyst for the one-pot synthesis of hexahydroquinoline-3-carboxamide derivatives by four-component reaction of arylaldehydes, dimedone, acetoacetanilide and ammonium acetate in high to excellent yield in ethanol at 50◦ c. the [2-mpy][p-tsa] catalyst was characterized via ft-ir, ^1h nmr and ^13c nmr spectroscopy. an environmentally benign procedure, four-component in one pot reaction, high yields and simple preparation of the catalyst are some advantages of this work.
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کلیدواژه
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2-Methylpyridinum p-toluenesulfonate ,Ionic liquid ,One-pot reaction ,Hexahydroquinoline-3-carboxamide
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آدرس
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islamic azad university, rasht branch, department of chemistry, Iran, islamic azad university, rasht branch, department of chemistry, Iran
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پست الکترونیکی
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mmokhtary@iaurasht.ac.ir
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Authors
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