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X-ray Structure of 2,6-Biphenyl-1,4-Diselenafulvene and its Reaction with Fe2(CO)9
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نویسنده
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منبع
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jordan journal of chemistry - 2007 - دوره : 2 - شماره : 3 - صفحه:247 -253
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چکیده
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2,6-biphenyl-1,4-diselenafulvene (1) was prepared by air oxidation of phc(identical)cse-. treatment of 1 with equimolar amounts of fe2(co)9 produced (μ3-se)2fe3(co)9 (2). compound 1 was characterized by elemental analysis, ir, 1h-, 13c{1h}-nmr spectroscopy and by x-ray structure determination, while compound 2 was characterized by elemental analysis, ir and ei- ms spectrometry.
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کلیدواژه
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Iron; Selenium; X-ray Structure; Deselenation; Alkyne; Metal carbonyl
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آدرس
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