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synthesis, characterization, and application of cofe₂o₄@sio₂@cptes@melamine nanoparticles as a magnetic catalyst for the synthesis of pyrazole derivatives
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نویسنده
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radhi obaid ammar ,shiri lotfi
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منبع
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journal of applied organometallic chemistry - 2024 - دوره : 4 - شماره : 3 - صفحه:178 -189
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چکیده
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In this work, an efficient procedure for the synthesis of pyrazole derivatives via a one-pot multi-component reaction of phenyl hydrazine, malanonitrile, and various aromatic aldehydes using cofe2o4@sio2@cptes@melamine as a magnetic nanocatalyst in water under room temperature conditions is reported. this nanocatalyst was synthesized in several steps and identified by various techniques including fourier-transform infrared (ft-ir), scanning electron microscopy (sem), energy dispersive x-ray (edx), thermogravimetric analysis (tga), x-ray diffraction (xrd), and vibrating sample magnetometer (vsm) techniques. the advantages of using this magnetic nanocatalyst in this research include easy synthesis, efficiency, non-toxicity, high-efficiency product production, short reaction time, and reusability.
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کلیدواژه
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5-amino-1h-pyrazole-4-carbonitrile ,phenylhydrazine ,malononitrile benzaldehyde
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آدرس
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ilam university, faculty of basic sciences, department of chemistry, iran, ilam university, faculty of basic sciences, department of chemistry, iran
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پست الکترونیکی
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lshiri47@gmail.com
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Authors
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