|
|
palladium supported on schiff base functionalized magnetite nanoparticles as an efficient catalyst for coupling reactions
|
|
|
|
|
نویسنده
|
balali masomeh ,bagherzadeh mojtaba ,nejat razieh ,keypour hassan
|
منبع
|
inorganic chemistry research - 2021 - دوره : 5 - شماره : 1 - صفحه:82 -93
|
چکیده
|
Palladium has been supported on 2-((3-(piperazin-1-yl) propylimino)methyl)phenol functionalized magnetite nanoparticles (denoted as fe3o4@sio2@l-pd(ii)). the supported pd was used as an active heterogeneous catalyst in the suzuki cross-coupling reaction under solvent-free conditions. this nanocatalyst could be facilely separated via magnetic concentration and the isolated catalyst exhibited longterm stability. easy work-up, high yield, recycling of the catalyst, low reaction times, non-toxicity of catalyst and solvent-free conditions as an environmentally benign procedure are the main merits of this protocol. the produced catalyst were characterized by xrd, ft-ir, xps, sem, tem, edax, vsm, tga and icp-oes.
|
کلیدواژه
|
palladium catalyst ,suzuki reaction ,magnetic separation ,solvent-free conditions
|
آدرس
|
hamedan university of technology, iran, sharif university of technology, chemistry department, iran, kosar university of bojnord, faculty of science, department of chemistry, iran, bu-ali sina university, faculty of chemistry, iran
|
پست الکترونیکی
|
bagherzadeh@sharif.edu;haskey1@yahoo.com
|
|
|
|
|
|
|
|
|
|
|
|
Authors
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|