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   sonochemical synthesis of novel nano flower lead(ii) metal-organic coordination polymer: a new precursor to produce nano-sized pbo  
   
نویسنده mirtamizdoust b. ,safari r. ,anbarteh s.
منبع inorganic chemistry research - 2017 - دوره : 1 - شماره : 2 - صفحه:171 -182
چکیده    The new nano flowerpb(ii) 1dmetal-organic chain {[pb(phen)(μ-ch3coo)]·(bf4)}n(1) (phen = 1,10-phenanthroline) was synthesized by a sonochemical irradiation assisted method. the compound was characterized by scanning electron microscopy (sem), elemental analysis, ft-ir spectroscopy, x-ray powder diffraction (xrpd) and single crystal x-ray analysis. the x-ray analysis reveals a 1dchain metal-organic coordination polymer structure for 1 thatis further extended into a 3d supramolecular structure by π-π and other labile interactions. the coordination number of the lead(ii) ions is determined was abouteight, pbf2n2o4. the lead oxide nanoparticles were prepared at 180 °c by the thermolysis of 1. the average diameter of the nanoparticles to be 27 nm. the size and morphology of the prepared pbo samples were further observed using sem.
کلیدواژه nanometal-organiccoordination polymer ,ultrasonicirradiation ,1dchain ,nano pbo
آدرس university of qom, faculty of science, department of chemistry, iran, university of qom, faculty of science, department of chemistry, iran, university of qom, faculty of science, department of chemistry, iran
پست الکترونیکی sanbarteh@gmail.com
 
     
   
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