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   Synthesis and Characterization of two Closed Side Oxadiazole ligands with their Related Complexes Cu( II ) and Pd(II)  
   
نویسنده mohamad Hikmat A.
منبع journal of university of anbar for pure science - 2009 - دوره : 3 - شماره : 1 - صفحه:- --
چکیده    The two oxadiazole new ligands of bis oxadiazol derivatives, have been synthesized by the reaction of 1, 2 - bis - [5=, 2= chloroethylsulphide)]1, 3, 4 - oxadaiazol - 2yl] ethane (l1)and1¯, 2¯ -bis- [5doublebarwedge, 2doublebarwedgechlororthyl sulphi)d],e oxadiazol-2yl] methane (l2.) with adibic acid in presence of ethnolic solution of potassium hydroxide. the mixture was refluxed for eight hours. the ligands were characterized using ir 1h.nmr13c-nmr and mass spectroscopies .the ( l3 ) was used to synthesize complexes with metals cu( ii ) and pd(ii ) . the complexes were studied and identified using ir, uv-vis spectra and molar conductivity, magnetic susceptibility and atomic absorption techniques. the results exhibited that all complexes have an octahedral structure.
کلیدواژه closed side ,ligands ,complexes
آدرس University of Salahaddin, Education of Science College, Iraq
پست الکترونیکی hikmatmohammed@yahoo.com
 
     
   
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