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   synthesis and characterization of cao catalyst obtained from achatina achatina and its application in biodiesel production  
   
نویسنده amusan oluwatobi o. ,louis hitler ,hamzat adejoke t. ,oyebanji oluwatomisin f. ,alagbe ayodeji t. ,magu thomas o.
منبع asian journal of nanoscience and materials - 2019 - دوره : 2 - شماره : 3 - صفحه:271 -277
چکیده    In this research study, achatina achatina shells was used as the source of raw material to produce calcium oxide which was used as a catalyst in the production of biodiesel. the main aim of this study was to investigate the effect of varying temperatures on the calcium oxide formed using a. achatina during the calcination process for their possible use as a heterogeneous catalyst in the production of biodiesel. the shells were first grinded and then calcinated at different temperatures ranging from 0 °c to 1000 °c. after calcination, the caco3 present in the a. achatina shell was converted to calcium oxide. the obtained calcium oxide was characterized using fourier transform infrared spectroscopy (ft-ir). the asymmetric stretching of the co3^2- (cm^-1) absorption was not proportional with the increasing temperature as it was observed over the plane vibrational modes of co3^2- (cm^-1). also, the o-h stretching band (cm^-1) at 100 °c and 800 °c had similar absorption values. pearson correlation revealed both negative and positive relationship between the absorption rate and the temperature, disclosed a significant difference at p<0.05. the calcined structure was examined using scanning electron microscope (sem) with a magnification of 10,000x. a more stabilized, uniform structure, and agglomerate into lumps were observed at 800 °c and 1000 °c. the results showed that, the a. achatina shell is a suitable catalyst in the production of biodiesel because it is readily available and has no adverse effect on the environment.
کلیدواژه achatina achatina ,calcium oxide ,heterogeneous catalyst ,biodiesel
آدرس university of ilorin, department of chemistry, nigeria, university of chinese academy of sciences, cas centre for excellence in nanoscience, national centre for nanoscience and technology, cas key laboratory for nanosystem and hierarchical fabrication, china, university of ilorin, department of chemistry, nigeria, university of ibadan, department of chemistry, nigeria, university of ilorin, department of chemistry, nigeria, university of chinese academy of sciences, institute of chemistry, cas key laboratory for green printing, china
 
     
   
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