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Synthesis, Spectroscopy and X-Ray Crystallography Structure of Pyridine 4-Carbaldehyde Semicarbazone Schiff Base Ligand
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نویسنده
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Mahmoudi Farzaneh ,Farhadi Saeed ,Dusek Michal ,Poupon Morgane
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منبع
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Advanced Journal Of Chemistry-Section A - 2020 - دوره : 3 - شماره : 4 - صفحه:534 -541
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چکیده
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In this work, pyridine 4-carbaldehye semicarbazone schiff base ligand (hl) was synthesized with condention of pyridine 4-carbaldehyde and semicarbazide hydrochloride in reflux method. the hl was characterized using the chn elemental analysis, ft-ir, uv-vis, and 1h nmr spectroscopy. the single crystals of hl prepared and used for the x-ray crystallography. single-crystal x-ray diffraction revealed that, hl crystallized in a triclinic system with the space group p-1. the ft-ir spectra and x-ray crystallography results suggested that the hl ligand is in keto form.
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کلیدواژه
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Semicarbazone ,Schiff Base Ligand ,Crystal Structure ,Spectroscopy
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آدرس
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Lorestan University, Department Of Chemistry, Iran, Lorestan University, Department Of Chemistry, Iran, Czech Academy Of Sciences, Institute Of Physics, Czech Republic, Czech Academy Of Sciences, Institute Of Physics, Czech Republic
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پست الکترونیکی
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poupon@fzu.cz
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Authors
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