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n,n,n’,n’-tetramethyln,n’-bis(sulfo)ethane-1,2- diaminium mesylate as a highly effective and dualfunctional catalyst for the synthesis of 1-thioamidoalkyl-2-naphthols
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نویسنده
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irannejad-gheshlaghchaei navid ,zare abdolkarim ,banaei alireza ,kaveh hamideh ,varavi nahid
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منبع
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chemical methodologies - 2020 - دوره : 4 - شماره : 4 - صفحه:400 -407
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چکیده
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N,n,n’,n’tetramethyln,n’bis(sulfo)ethane1,2diaminium mesylate ([tmbsed][oms]2) is used as a highly efficient and dualfunctional catalyst for the onepot multicomponent condensation of 2naphthol with arylaldehydes and thioacetamide under green, mild (70 °c), and solventfree conditions. in this reaction, 1thioamidoalkyl2naphthols are produced in high to excellent yields and in relatively short reaction times. in this reaction, products are identified by analysis of its 1h nmr, 13c nmr, and ftir data. moreover, a plausible mechanism based on dualfunctionality of the catalyst was proposed.
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کلیدواژه
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n' ,n'-tetramethyl-n ,n'-bis(sulfo)ethane-1 ,2-diaminium mesylate ([tmbsed][oms]2) ,thioacetamide ,1-thioamidoalkyl-2-naphthol ,multi-component reaction ,dicationic ionic liquid ,dual-functional catalyst
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آدرس
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payame noor university, department of chemistry, iran, payame noor university, department of chemistry, iran, payame noor university, department of chemistry, iran, payame noor university, department of chemistry, iran, payame noor university, department of chemistry, iran
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پست الکترونیکی
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nahid.varavi9@gmail.com
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Authors
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