>
Fa   |   Ar   |   En
   electrochemical behaviour of 5-methoxy-5,6-bis(3-nitropheyl-4,5-dihydro-1,2,4-triazine-3(2h))-thione in presence of salicylaldehyde on zinc cathode with surface morphology and biological activity  
   
نویسنده srikanta sasigolli annappa ,naik putta naik parmeswara ,krishanamurthy ganga naik
منبع asian journal of green chemistry - 2020 - دوره : 4 - شماره : 2 - صفحه:149 -158
چکیده    this paper presents an innovative, green and organic electro synthesis in order to prepare schiff base product by the reduction of 5-methoxy-5,6-bis (3-nitropheyl-4,5-dihydro-1,2,4-triazine-3(2h))-thione followed by the condensation on zinc cathode in aqueous alkaline ethanol media in the presence of salicylaldehyde at room temperature. the main characteristic of this proposal is the electro-reduction and electro-condensation. the bulk electrolysis at constant potential was performed in a three-electrode undivided cell in order to prepare schiff base. in this sense, good yields and easy purification were achieved. results indicate that the reduction produced high current in the cell and succeeded a green chemistry process. products were characterized by ir, nmr (1h, 13c), and sem.
کلیدواژه electrolysis ,surface morphology ,organic electro-synthesis ,cathode
آدرس sahyadri science college, department of chemistry, india, sahyadri science college, department of chemistry, india, sahyadri science college, department of chemistry, india
پست الکترونیکی gkmnaiksahyadri@gmail.com
 
 

Copyright 2015
Islamic World Science Citation Center
All Rights Reserved