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   determination of diazinon in environmental samples using modified multi-walled carbon nanotubes as pipette-tip solid phase extraction sorbent  
   
نویسنده rezaei kahkha mohammad reza ,kaykhaii massoud ,shafee-afarani mahdi ,rezaei kahkha batool
منبع iranian journal of analytical chemistry - 2017 - دوره : 4 - شماره : 2 - صفحه:10 -16
چکیده    In this work, a microextraction technique based on pipette tip solid-phase extraction was used for preconcentration and determination of diazinon. carbon nanotube functionalized by zinc sulfide and ethylene glycol was used as sorbent. determination of diazinon was performed using high performance liquid chromatography and uv detection. important parameters that influence the extraction efficiency (i.e. ph, amount of adsorbent, extraction time, salt addition, volumes of sample and eluting solvent and number of aspirating/dispensing cycles for both solvent and sample) were investigated and optimized. results were showed that method was validated over the range of 0.50 - 100.0 μg l^-1. repeatability was satisfactory, bellow 3.78% for 5 replicate measurements of 20 μg l^-1 of diazinon. the limit of detection of this method is 0.03 μg l^-1 with an enrichment factor of 100 and short extraction time of 8.5 min, which confirmed suggested method is a reliable and accurate for extraction and preconcentration of diazinon.
کلیدواژه carbon nanotubes ,diazinon ,pipette tip ,preconcentration ,solid phase extraction
آدرس zabol university of medical sciences, faculty of health, department of environmental health engineering, ایران, university of sistan and baluchestan, faculty of sciences, department of chemistry, ایران, university of sistan and baluchestan, department of material engineering, ایران, kerman university of medical sciences, department of occupational health engineering, ایران
پست الکترونیکی batoool.rezaei.k@gmail.com
 
   اندازه‌گیری دیازینون در نمونه‌های محیطی با استفاده از نانولوله‌های اصلاح‌شده کربنی با استفاده از سرسمپلر  
   
Authors رضایی‌کهخا محمدرضا ,کیخوایی مسعود ,شفیع آفرانی مهدی ,رضایی کهخا بتول
  
 
 

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