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magnetic solid ‒ phase extraction of trace amounts of nickel in food samples using polydopamine coated fe3o4 nanoparticles
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نویسنده
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nekoeinia mohsen ,yousefinejad saeed ,abdi mohammad reza ,ebrahimpour behnam
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منبع
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iranian journal of analytical chemistry - 2017 - دوره : 4 - شماره : 2 - صفحه:1 -9
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چکیده
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A simple and a green methodology has been developed for the preconcentration of ni^2+ based on the adsorption of its dimethylglyoximate complex on polydopamine coated fe3o4 nanoparticles. the adsorbed complex was easily desorbed using 1.0 ml of chcl3 and the concentration of nickel was determined by uv-vis spectrophotometry. the effects of ph, sorbent mass, extraction time on the sorption of nickel dimethylglyoximate complex were investigated using box–behnken design. in optimal experimental conditions, a wide linear range of 5.0-600.0 μg/l with detection limit of 1.49 μg/l was obtained. the proposed method was applied for extraction and preconcentration of ni^2+ in various food samples and the results were compared with the official aoac method.
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کلیدواژه
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nickel; polydopamine; magnetic solid‒phase extraction; nanosorbents; dimethylglyoxime
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آدرس
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payame noor university, department of chemistry, ایران, shiraz university of medical sciences, school of health, department of occupational health engineering, ایران, payame noor university, department of chemistry, ایران, tarbiat modares university, department of chemistry, ایران
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پست الکترونیکی
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ebrahim_pour1@yahoo.com
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استخراج فاز جامد مغناطیسی مقادیر ناچیز نیکل در نمونههای مواد غذایی با نانوذرات اکسید آهن پوشش داده شده با پلی دوپامین
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Authors
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نکوئی نیا مسعود ,یوسف نژاد سعید ,عبدی محمدرضا ,ابراهیم پور بهنام
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