|
|
Influence of Zn/Fe molar ratio on optical and magnetic properties of ZnO and ZnFe2O4 nanocrystal as calcined products of layered double hydroxides
|
|
|
|
|
نویسنده
|
ahmed a.a.a. ,talib z.a. ,hussein m.z. ,flaifel m.h. ,al-hada n.m.
|
منبع
|
journal of spectroscopy - 2014 - دوره : 2014 - شماره : 0
|
چکیده
|
The coprecipitation method has been used to synthesize layered double hydroxide (zn-fe-ldh) nanostructure at different zn2+/fe3+ molar ratios. the structural properties of samples were studied using powder x-ray diffraction (pxrd). ldh samples were calcined at 600°c to produce mixed oxides (zno and znfe2o4). the crystallite size of mixed oxide was found in the nanometer scale (18.1 nm for znfe2o 4 and 43.3 nm for zno). the photocatalytic activity of the calcination products was investigated using ultraviolet-visible-near infrared (uv-vis-nir) diffuse reflectance spectroscopy. the magnetic properties of calcined ldhs were investigated using a vibrating sample magnetometer (vsm). the calcined samples showed a paramagnetic behavior for all zn2+/fe 3+ molar ratios. the effect of molar ratio on magnetic susceptibility of the calcined samples was also studied. © 2014 abdullah ahmed ali ahmed,et al.
|
|
|
آدرس
|
department of physics,faculty of applied science,thamar university,p.o. box 87246, Yemen, Universiti Putra Malaysia, Malaysia, Universiti Putra Malaysia, Malaysia, Universiti Kebangsaan Malaysia, Malaysia, Universiti Putra Malaysia, Malaysia
|
|
|
|
|
|
|
|
|
|
|
|
|
|
Authors
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|