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Comparative studies on conventional and ultrasound-assisted synthesis of novel homoallylic alcohol derivatives linked to sulfonyl dibenzene moiety in aqueous media
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نویسنده
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mady m.f. ,el-kateb a.a. ,zeid i.f. ,jorgensen k.b.
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منبع
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journal of chemistry - 2013 - دوره : 2013 - شماره : 0
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چکیده
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Novel homoallylic alcohols incorporating sulfone moieties were synthesized by the treatment of different carbonyl compounds with allylic bromides in aqueous media via sonochemical barbier-type reaction conditions. sulfonation of α-bromoketones with sodium benzenesulfinate in presence of cui/2,6-lutidine rapidly gave β-keto-sulfones in good yields. in general,ultrasound irradiation offered the advantages of high yields,short reaction times,and simplicity compared to the conventional methods. the structures of all the compounds were confirmed by analytical and spectral data. © 2013 mohamed f. mady et al.
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آدرس
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department of mathematics and natural sciences,faculty of science and technology,university of stavanger,4036 stavanger,norway,department of green chemistry,national research centre,dokki, Egypt, department of green chemistry,national research centre,dokki, Egypt, chemistry department,faculty of science,menoufia university,shebin el-koam, Egypt, department of mathematics and natural sciences,faculty of science and technology,university of stavanger, Norway
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Authors
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