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Synthesis,crystal structure,and fungicidal activity of 5-(4-cyclopropyl-5-((3-fluorobenzyl)thio)-4 H -1,2,4-triazol-3-yl)-4-methyl-1,2,3-thiadiazole
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نویسنده
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liu x.-h. ,weng j.-q. ,tan c.-x.
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منبع
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journal of chemistry - 2013 - دوره : 2013 - شماره : 0
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چکیده
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A new 1,2,3-thiadiazole compound was synthesized and characterized. the crystal structure of the title compound (c15h14fn 5s2,mr = 347.43) has been determined by single-crystal x-ray diffraction. the crystal is of triclinic,space group p-1 with a=7.0490(14),b=9.0212(18),c=12.799(3) å,α = 89.97(3)°,β = 82.27(3)°,γ = 73.17(3)°,v = 771.3(3) å3,z = 2,f(000) = 360,dc = 1.496 g/cm3,= 0.036 mm-1,the final r1 = 0.0358,and wr2 = 0.0986 for 2204 observed reflections with i>2σ(i). a total of 5697 reflections were collected,of which 2719 were independent (rint=0.0028). the herbicidal activity of title compound was determined; the results showed that the title compound displayed excellent fungicidal activity. © 2013 xing-hai liu et al.
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آدرس
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college of chemical engineering and materials science,zhejiang university of technology, China, college of chemical engineering and materials science,zhejiang university of technology, China, college of chemical engineering and materials science,zhejiang university of technology, China
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Authors
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