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Synthesis and single crystal X-ray structure of new (2 E)-2-[3-(1 H -Imidazol-1-yl)-1-phenylpropylidene]- N -phenylhydrazinecarboxamide
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نویسنده
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attia m.i. ,ghabbour h.a. ,el-azzouny a.a. ,al-deeb o.a. ,almutairi m.s. ,fun h.-k.
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منبع
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journal of chemistry - 2013 - دوره : 2013 - شماره : 0
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چکیده
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Synthesis,spectroscopic characterization and x-ray crystal structure of a new (2e)-2-[3-(1h-imidazol-1-yl)-1-phenylpropylidene]-n- phenylhydrazinecarboxamide (4) are reported. the stereochemistry of the title compound 4,c19h19n5o,about the imine bond [1.296 (4) å] was assigned to have (e)-configuration. in the urea moiety,the n-h entities are trans to each other,and one of these forms is an intramolecular n-hh hydrogen bond. the compound crystallizes in the monoclinic space group p21/c with a = 5.8093 (2) å,b = 20.5575 (6) å,c = 14.0355 (5) å,α = 90.00°,β = 97.365° (2),γ = 90.00°,v = 1662.36 (10) å3,and z = 4. the molecules are packed in crystal structure by weak intermolecular hydrogen interactions. © 2013 mohamed i. attia et al.
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آدرس
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department of pharmaceutical chemistry,college of pharmacy,king saud university,p.o. box 2457,riyadh 11451,saudi arabia,medicinal and pharmaceutical chemistry department,pharmaceutical and drug industries research division,national research centre,dokki, Egypt, department of pharmaceutical chemistry,college of pharmacy,king saud university,p.o. box 2457, Saudi Arabia, medicinal and pharmaceutical chemistry department,pharmaceutical and drug industries research division,national research centre,dokki, Egypt, department of pharmaceutical chemistry,college of pharmacy,king saud university,p.o. box 2457, Saudi Arabia, department of pharmaceutical chemistry,college of pharmacy,king saud university,p.o. box 2457, Saudi Arabia, department of pharmaceutical chemistry,college of pharmacy,king saud university,p.o. box 2457, Saudi Arabia
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Authors
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