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Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine
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نویسنده
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gao s. ,qu h.-t. ,ye f. ,fu y.
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منبع
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journal of chemistry - 2015 - دوره : 2015 - شماره : 0
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چکیده
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A new compound,n-dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2h-1,4-benzoxazine,was synthesized and characterized. the crystal structure of the title compound (c11h10cl3no2,mr = 294.55) has been determined by single-crystal x-ray diffraction. the crystal belongs to monoclinic,space group p21/c,with a = 6.7619 (14),b = 24.866 (5),c = 9.737 (3) å,α = 90.00,β = 130.982 (18),γ = 90.00 °,v = 1235.9 (5) å3,z = 4,dx = 1.583 mg/cm3,λ(mo ka) = 0.71073 å,f (000) = 600,μ = 0.729 mm-1,r = 0.0476,and wr = 0.1274 for 2217 reflections with i > 2 σ (i). © 2015 shuang gao et al.
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آدرس
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college of science,northeast agricultural university,harbin, China, college of science,northeast agricultural university,harbin, China, college of science,northeast agricultural university,harbin, China, college of science,northeast agricultural university,harbin, China
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Authors
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