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a new precursor for preparation of magnetite (fe3o4) nanoparticles
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نویسنده
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kaikhosravi mohammad ,hadadzadeh hassan ,behnamfar mohammad-taghi
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منبع
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journal of particle science and technology - 2015 - دوره : 1 - شماره : 2 - صفحه:65 -72
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چکیده
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An anionic fe(ii) complex, (bmim)4[fe(cn)6] (where bmim is 1butyl3methylimidazolium), was synthesized in ionic liquid [bmim][pf6] under reflux condition. the complex was characterized by elemental analysis and spectroscopic methods. the magnetite (fe3o4) nanoparticles were prepared by the hydrothermal and solvothermal (in ionic liquid [bmim][pf6]) methods from (bmim)4[fe(cn)6] as a precursor. the nanoparticles were characterized by xray diffraction (xrd), ftir, and scanning electron microscopy (sem). the results show that the preparation of magnetite using the solvothermal method in [bmim][pf6] has more advantages such as smaller size and high purity.
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کلیدواژه
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ionic liquid ,solvothermal ,1-butyl-3-methylimidazolium hexafluorophosphate ,magnetite ,hydrothermal
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آدرس
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isfahan university of technology, department of chemistry, ایران, isfahan university of technology, department of chemistry, ایران, isfahan university of technology, department of chemistry, ایران
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پست الکترونیکی
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behnam10@gmail.com
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Authors
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