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Determination of Zinc Ions in Environmental Samples by Dispersive Liquid- Liquid Micro Extraction and Atomic Absorption Spectroscopy
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نویسنده
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arabi f. ,emami meibodi a. ,aflaki f.
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منبع
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journal of chemical health risks - 2012 - دوره : 2 - شماره : 3 - صفحه:13 -16
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چکیده
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In this work preconcentration of the zn ions was investigated in water sample by dispersive liquid- liquid micro extraction (dllme) using chloroform as an extraction solvent, methanol as a disperser solvent and 8-hydroxyquinoline as a chelating agent. the determination of extracted ions was done by graphite furnace atomic absorption spectrometry. the influence of various analytical parameters including ph, extraction and disperser solvent type and volume and concentration of the chelating agent on the extraction efficiency of analyses was investigated. after extraction, the enrichment factor was 26 and the detection limit of the method was 0.0033 μg l^-1 and the relative standard deviations (r.s.d) for five determinations of 1 ng/ml zn were 7.41%.
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کلیدواژه
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Dispersive liquid- liquid micro extraction (DLLME) ,Graphite furnace atomic absorption spectrometry ,Zinc ,water samples
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آدرس
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islamic azad university, saveh branch, department of chemistry, ایران, islamic azad university, karaj branch, department of chemistry, ایران, nuclear science and technology research institute, nuclear science research school, ایران
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Authors
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