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one-pot solvent-free synthesis of pyranonaphthoquinone-fused spirooxindoles catalyzed by sba-il
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نویسنده
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mohammadi ziarani ghodsi ,mollabagher hoda ,lashgari negar ,badiei alireza
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منبع
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scientia iranica - 2018 - دوره : 25 - شماره : 6-C - صفحه:3295 -3304
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چکیده
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In this research, ionic liquid modified sba-15 mesoporous material (sba-il) as a recyclable, heterogeneous catalyst efficiently catalyzed the synthesis of pyranonaphthoquinone-fused spirooxindoles through the one-pot three-component reaction of isatin derivatives, activated methylene reagents, and 2-hydroxy-1,4-naphthoquinone. the reactions were performed under microwave irradiation and solvent-free conditions. the synthesized sba-il was characterized by sem, ft-ir, nitrogen adsorption-desorption, and thermogravimetric analyses. excellent chemical yield, short reaction time, mild reaction condition, easy workup procedures, and reusability of catalyst are noteworthy advantages of this protocol.
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کلیدواژه
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sba-il;multicomponent reaction;spirooxindole;isatin;mesoporous silica;heterogeneous catalyst
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آدرس
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alzahra university, department of chemistry, iran, alzahra university, department of chemistry, iran, alzahra university, department of chemistry, iran, university of tehran, school of chemistry, college of science, iran
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پست الکترونیکی
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abadiei@khayam.ut.ac.ir
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Authors
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