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magnetic investigation of microwave synthesized and thermal stable poly vinyl alcohol-cobalt ferrite nanocomposites
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نویسنده
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karbasi matin ,maghazeii farnaz ,ghanbari davood
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منبع
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journal of nanostructures - 2019 - دوره : 9 - شماره : 2 - صفحه:365 -375
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چکیده
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Cofe2o4 nanoparticles was prepared using heating in various times by simple microwave method at power about 600w. water, ethylene glycol and their combination were used as solvent. x-ray diffraction pattern (xrd) analysis was performed for evaluation of structural characterization of samples. we also used scanning electron microscopy (sem) to evaluate the effects of various parameters of heating time and solvent type on mean grain size and nanostructure of the samples. our results showed that with changing of these parameters, we can control the nanostructure and grain size of prepared samples. in addition, we produced polymeric nanocomposite of pva/cofe2o4 using polyvinyl alcohol films. the thermal stability of it in comparison to pva polymer was assessed by thermal gravimetric analysis (tga). also the nanostructures of polymer nanocomposite were analyzed by sem. to evaluate the magnetic parameters of samples, vibrating sample magnetometer (vsm) analysis were done. also the spectrum of pva polymer and polymer nanocomposite were drawn by ft-ir. our results confirmed that the nanostructures, magnetic behavior and thermal stability of the prepared nanocomposite are acceptable for needed applications.
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کلیدواژه
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cobalt ferrite nanoparticles ,magnetic behavior ,nanostructure ,polymer nanocomposite ,thermal stability
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آدرس
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islamic azad university, arak branch, iran, islamic azad university, arak branch, science faculty, mathematics and physics department, iran, arak university of technology, department of science, iran
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پست الکترونیکی
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ghanbarichemist@gmail.com
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Authors
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