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Determination of the absolute configuration of new piperidin-4-one derivative from pellacalyx saccardianus by NOESY spectroscopy
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نویسنده
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abed s.a. ,sirat h.m.
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منبع
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jurnal teknologi - 2016 - دوره : 78 - شماره : 3-2 - صفحه:15 -18
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چکیده
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A new alkaloid,pellacalyxin was isolated from the leaves of pellacalyx saccardianus of rhizophoraceae family. pellacalyxin was analyzed using nuclear overhauser spectroscopy (noesy) nuclear magnetic resonance (nmr) technique to determine the absolute configuration. the analysis of absolute configuration of pellacalyxin was supported by x-ray crystallography.1h-1h noesy nmr spectroscopy exhibited that pellacalyxin possesses two chiral centers (3s) and (6r). © 2016 penerbit utm press. all rights reserved.
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کلیدواژه
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Absolute configuration; NOESY spectroscopy; Pellacalyx saccardianus; Pellacalyxin; X-ray crystallography
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آدرس
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department of chemistry,universiti teknologi malaysia,utm,johor bahru,johor,malaysia,department of pharmacognosy,college of pharmacy,kerbala university,kerbala, Iraq, department of chemistry,universiti teknologi malaysia,utm,johor bahru,johor, Malaysia
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Authors
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