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solid state preparation of cdo nano-particles by thermolysis of a precursor as compacted nanosheet
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نویسنده
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rashidi ranjbar z. ,sheikhshoaie i. ,bagheri z.
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منبع
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international journal of nano dimension - 2014 - دوره : 5 - شماره : 4 - صفحه:409 -413
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چکیده
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A novel complex of cadmium (ii) [cdl0.5(no3)(h2o)](1), l= n,n-bis (o-hydroxyacetophenone) ethylene diamine, have been synthesized as single crystal and nano size. compound 1 in nano size was obtained under sonochemical irradiation and has been characterized by ir, 1hnmr spectroscopy, x-ray powder diffraction (xrd) and scanning electron microscopy (sem). the gray single crystal of compound 1 has been synthesized by slow evaporation and characterized by ir, 1hnmr spectroscopy. then, compound 1 in nano size was used as initial reagent to obtain nano-particles of cadmium (ii) oxide at 673 k by direct calcination. the obtained cdo nano-particles were characterized by xrd pattern as well as sem images.
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کلیدواژه
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nanoparticle ,cdo ,sonochemistry ,cadmium (ii) complex ,thermolysis
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آدرس
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shahid-bahonar university of kerman, department of chemistry, ایران, shahid-bahonar university of kerman, department of chemistry, ایران, shahid-bahonar university of kerman, department of chemistry, ایران
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Authors
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