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   synthesis and characterization of silver and gold nano-structures on chitosan-porous anodic alumina nano-composite  
   
نویسنده qayyum somia ,mehmood mazhar ,mirza muhammad aslam ,ashraf sumaira ,ahmed zahoor ,tanvir tauseef ,choudhary muhammad aziz ,iqbal masood ,nisar faria ,nisa zaib un
منبع iranian journal of chemistry and chemical engineering - 2019 - دوره : 38 - شماره : 6 - صفحه:31 -44
چکیده    This study was designed to probe the fabrication of unique silver and gold nano-structures engaging a self-designed chitosan-porous anodic alumina nano-composite as template. porous anodic alumina have been manufactured by di-step aluminum anodization in oxalic acid electrolytic bath. the surface properties of porous anodic alumina were reinforced by chitosan neutralized in sodium hydroxide. multifarious nano-morphologies of silver as well as gold nano-structures were observed. furthermore, the long chitosan biopolymer chains were degraded by γ-irradiations and the same procedure was employed for modification of porous anodic alumina with γ-degraded chitosan. the morphologies of fabricated silver and gold nano-structures were investigated by scanning electron microscopy, while their composition was evaluated with the help of energy dispersive x-ray spectroscopy. x-ray diffraction study exposed face centered cubic phase for both silver and gold nano-structures. reflection mode uv-vis spectroscopy was used to ascertain reflection grooves in the absorption range of silver and gold nano-structures respectively. the technique does not involve any harmful reagent and show different selectivity than methods in general practice. the achieved results apprised that the fabricated nano-structures offer the advantages of biocompatibility and eco-friendliness for numerous biomedical uses.
کلیدواژه porous anodic alumina; di-step aluminum anodization; chitosan; nano-composite; gold and silver nano-structures
آدرس mirpur university of science and technology (must), department of chemistry, pakistan, pakistan institute of engineering and applied sciences (pieas), department of metallurgy and materials engineering, pakistan, mirpur university of science and technology (must), department of chemistry, pakistan, pakistan institute of engineering and applied sciences (pieas), department of metallurgy and materials engineering, pakistan, mirpur university of science and technology (must), department of chemistry, pakistan, pakistan institute of engineering and applied sciences (pieas), department of metallurgy and materials engineering, pakistan, mirpur university of science and technology (must), department of chemistry, pakistan, mirpur university of science and technology (must), department of chemistry, pakistan, mirpur university of science and technology (must), department of chemistry, pakistan, mirpur university of science and technology (must), department of chemistry, pakistan
 
     
   
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