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Controlled Crystallization of LTA Zeolitic Nanoparticles from a Clear Solution Using Organic Template
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نویسنده
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Esmaeili Nazila ,Kazemian Hossein ,Bastani Dariush
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منبع
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iranian journal of chemistry and chemical engineering - 2011 - دوره : 30 - شماره : 2 - صفحه:9 -14
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چکیده
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Lta zeolite nanoparticles was successfully synthesized from clear solution under controlled conditions using hydrothermal method using tetramethyl ammonium hydroxide as a structural directing agent. the as-synthesized lta zeolite particles were characterized by powder x-ray diffraction (xrd) analysis, scanning electron microscopy (sem), fourier transform infrared (ft-ir) spectroscopy, energy dispersive x-ray (edx) analysis and surface area measuring technique of brunauer, emmett and teller (bet). xrd patterns and ft-ir spectra were ascertained the formation of pure crystalline phase of 4a (i.e. lta) zeolite.sem micrograph was shown particles size in the range of 60 -170 nm with uniform morphology.the si /al ratio of the as-synthesized zeolite nanoparticles was 1.66 with a bet surface area of 421 m2/g
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کلیدواژه
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LTA zeolite ,Nanoparticle ,Hydrothermal synthesis ,Controlled crystallization
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آدرس
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sharif university of technology, Faculty of Chemical and Petroleum Engineering, ایران, University of Western Ontario (UWO), Faculty of Engineering, Department of Chemical and Biochemical Engineering, CANADA, sharif university of technology, Faculty of Chemical and Petroleum Engineering, ایران
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پست الکترونیکی
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hossein.kazemian@uwo.ca
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Authors
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