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Spectral characterization and crystal structure of 2-amino-N'-[(1Z)-1-(4-chlorophenyl)ethylidene]-benzohydrazide
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نویسنده
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arfan m. ,khan r. ,tavman a. ,saba s.
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منبع
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journal of saudi chemical society - 2016 - دوره : 20 - شماره : 1 - صفحه:40 -44
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چکیده
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The crystal structure of 2-amino-n'-[(1z)-1-(4-chlorophenyl)ethylidene]benzohydrazide (i) is determined by x-ray diffraction at room temperature. the structure of i also was characterized by elemental analysis,mass,ft-ir and nmr spectroscopic techniques. the compound crystallizes in triclinic system,and space group is p1-. unit-cell dimensions are the following: a = 7.05380(10) å,b = 7.65490(10) å,c = 13.7094(4) å,v = 694.01(2) å3,z = 2. the title compound is nearly planar and has intermolecular n-h...o hydrogen bonding. according to the spectral data,i exhibits an amide-iminol tautomerism. © 2012 king saud university. production and hosting by elsevier b.v.
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کلیدواژه
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Benzohydrazide; Chlorophenyl-ethylidene; Crystal structure; Spectroscopy
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آدرس
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institute of chemical sciences,university of peshawar, Pakistan, institute of chemical sciences,university of peshawar, Pakistan, istanbul university,faculty of engineering,chemistry department,avcilar, Turkey, institute of chemical sciences,university of peshawar, Pakistan
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Authors
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